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¾ Establishing the extent of severity of a disease ¾ Assessing the course and stage of clinical condition ¾ Differential diagnosis of many diseases ¾ Monitoring response to therapy

 


TURBIDIMETRY

Introduction

Diagnosis is a decision point. The decision is the intention

to treat. It is the point at which sufficient evidence has

been accumulated to state, beyond reasonable doubt, that

the patient is or is not suffering from a particular disease.

Laboratory tests remain one of the mainstays on which

the clinicians rely for diagnosis and management of the

patient. Laboratory tests are indicated for:

1. Detection

The presence or absence of a particular substance, e.g.

testing for infectious diseases like Venereal Diseases

Research Laboratory (VDRL), hepatitis B surface antigen

(HBsAg).

2. Quantification

Accurately determining the concentration of a particular

substance as an aid to diagnosis or differential diagnosis

(e.g. concentration of CRP in differential diagnosis of viral

and bacterial infections) and for establishing the extent

700 Concise Book of Medical Laboratory Technology: Methods and Interpretations of the clinical condition (e.g. IgA in measuring disease

severity).

3. Monitoring

The course of clinical condition or response to therapy.

4. Prognosis

For predicting the probability of occurrence of a disease/

disorder (e.g. microalbuminuria for predicting diabetic

nephropathy) or predicting the outcome of a disease/

disorder.

Microscopy, biochemical assays, microbiology

procedures, and immunoassays are various techniques

that fulfil the requirements of routine laboratory tests to

meet the needs of the clinicians.

Certain clinical analytes can be measured by specific

techniques only, whereas for the measurement of certain

analytes options exist for selecting the techniques of

measurement. For example, urinary albumin can be

measured by biochemical methods such as pyrogallol

red or coomassie blue. But for the diagnosis of microalbuminuria, a condition where urinary excretion of

albumin is in the range of 30–300 mg/L, the accuracy

of the measurements by biochemical methods is

questionable because these methods also react with other

proteins in addition to albumin which are frequently

found to be present in urine. Immunochemical methods

(immunoassays) which are more sensitive and specific

have a distinct advantage and, hence, are preferred.

Immunoassays

Immunoassays are assays that detect the presence of an

antigen in the human body with the help of an antibody

or detect the presence of an antibody with the help of an

antigen. In this text for simplicity, all further information

provided is based on considering antibody as a reagent to

detect antigen in the human body fluids.

The first reported immunoassays were homogeneous.

They are attributed to Kraus (1897), who coined the term

‘precipitin’ for the precipitate formed upon mixing an

antigen and an antibody.

Meyer in 1922, employed sheep erythrocytes to serve

as a label and conjugated human immunoglobulin to

them. Anti-immunoglobulin antibodies appearing in

rheumatoid arthritis patients were shown to cause visible

clumping of these erythrocytes. This method was known

as hemagglutination.

Singer and Plotz replaced the erythrocytes with latex

particles, which were easier to standardize, and these

assays are popularly known as latex agglutination

tests. High degree of sensitivity for a wide variety

of antigens/antibodies, which can be detected by

these latex agglutination assays, has promoted their

usage worldwide for screening since, 1956 in clinical

laboratories. The simplicity of performance and

obviating the need for equipments, have made these

assays extremely popular.

The need for quantitative estimation, and higher

sensitivity led to the development of radioimmunoassays

(RIA) first in 1959 by Berson and Rosalyn Yalow. The first

RIA developed was used to detect and quantify insulin.

Since then immunoassays have been used to detect and

quantify a variety of molecules native to humans such as

proteins, hormones as well as foreign molecules such as

bacteria, viruses and parasites.

Qualitative Immunoassays

Qualitative immunoassay techniques provide test results,

which only help to identify or indicate the presence of

analytes. Various techniques for qualitative detection of

antigens have been in use, which include latex agglutination, passive gel diffusion, IEP and Western blotting.

These techniques at the best can give a semiquantitative

or comparative information about analytes under assay.

Single immunodiffusion technique uses the diffusion

of an antigen into agar impregnated with antibody.

Double immunodiffusion technique allows the direct

comparison of two or more test materials providing a

simple and direct method for determining whether the

antigens in the test specimens are identical, cross-reactive,

or non-identical. Immunoelectrophoresis has been used

over the years for detection of several different antigens

present in a common solution. The latex agglutination

assays though simple to use are subject to variations in

results as the interpretation pattern between negative and

weakly reactive samples may vary between laboratory to

laboratory and person to person.

Lower sensitivity for many analytes and the need for

correct quantification of analytes for:

¾ Effective monitoring of disease

¾ For differential diagnosis to aid correct therapy,

have created the need for more sensitive and precise

quantitative immunoassays.

Quantitative Immunoassays

Quantitative results of immunoassays are extremely useful

in:

¾ Establishing the extent of severity of a disease

¾ Assessing the course and stage of clinical condition

¾ Differential diagnosis of many diseases

¾ Monitoring response to therapy

¾ Accurate prognosis of disease.

Diagnostic Immunology 701

Various techniques have been used to develop

quantitative methods that include radial immunodiffusion

(RID) and electroimmunoassays, turbidimetric and

nephelometric assays and labeled immunochemical assays.

The RID and electroimmunoassay (rocket electrophoresis)

though reliable, are slow, relatively involvement intensive,

and expensive. This limits their usage in routine laboratories.

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